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|Title:||Electrochemical cell for neutron reflectometry studies of the structure of ionic liquids at electrified interface|
|Publisher:||American Institute of Physics|
|Citation:||Lauw, Y., Rodopoulos, T., Gross, M., Nelson, A., Gardner, R., & Home, M. D. (2010). Electrochemical cell for neutron reflectometry studies of the structure of ionic liquids at electrified interface. Review of Scientific Instruments, 81(7), 074101. doi:10.1063/1.3455178|
|Abstract:||We describe the design and use of a closed three-electrode electrochemical cell for neutron reflectometry studies of the structure of the electrical double-layer in ionic liquids. A transparent glass counter electrode was incorporated to allow easy monitoring of any gas bubbles trapped in the cell. A 100 mm diameter silicon wafer polished to 0.1 nm rms roughness coated with gold over a chromium adhesion layer was used as the working electrode. The utility of the cell was demonstrated during neutron reflectometry measurements of the ultrahigh purity ionic liquid 1-butyl-1-methylpyrrolidinium bis(trifluoromethylsulfonyl)imide ([C4mpyr][NTf2]) at two different applied potentials. © 2010, American Institute of Physics|
|Gov't Doc #:||2561|
|Appears in Collections:||Journal Articles|
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