Please use this identifier to cite or link to this item: https://apo.ansto.gov.au/dspace/handle/10238/8128
Title: Microstructure and texture analysis of δ-hydride precipitation in Zircaloy-4 materials by electron microscopy and neutron diffraction
Authors: Wang, ZY
Garbe, U
Li, HJ
Wang, YB
Studer, AJ
Sun, GG
Harrison, RP
Liao, XZ
Vicente Alvarez, MA
Santisteban, JR
Kong, C
Keywords: Microstructure
Zircaloy
Neutron diffraction
Microstructure
Electron sources
Zirconium alloys
Issue Date: 1-Jan-2014
Publisher: International Union of Crystallography
Citation: Wang, Z., Garbe, U., Li, H., Wang, Y., Studer, A. J., Sun, G., Harrison, R. P., Liao, X., Vicente Alvarez, M. A., Santisteban, J. R., & Kong, C. (2014). Microstructure and texture analysis of d-hydride precipitation in Zircaloy-4 materials by electron microscopy and neutron diffraction. Journal of Applied Crystallography, 47(1), 303-315. doi:10.1107/S1600576713031956
Abstract: This work presents a detailed microstructure and texture study of various hydrided Zircaloy-4 materials by neutron diffraction and microscopy. The results show that the precipitated δ-ZrH1.66 generally follows the δ (111)//α(0001) and δ [110]//α[1120] orientation relationship with the α -Zr matrix. The δ-hydride displays a weak texture that is determined by the texture of the α-Zr matrix, and this dependence essentially originates from the observed orientation correlation between α-Zr and δ-hydride. Neutron diffraction line profile analysis and high-resolution transmission electron microscopy observations reveal a significant number of dislocations present in the δ-hydride, with an estimated average density one order of magnitude higher than that in the α-Zr matrix, which contributes to the accommodation of the substantial misfit strains associated with hydride precipitation in the α -Zr matrix. The present observations provide an insight into the behaviour of δ-hydride precipitation in zirconium alloys and may help with understanding the induced embrittling effect of hydrides.© 2014 International Union of Crystallography.
Gov't Doc #: 7675
URI: http://dx.doi.org/10.1107/S1600576713031956
http://apo.ansto.gov.au/dspace/handle/10238/8128
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